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Beilstein J. Org. Chem. 2010, 6, 960–965, doi:10.3762/bjoc.6.107
Graphical Abstract
Scheme 1: Synthesis of R-3 and S-3.
Figure 1: Concentration-dependent 1H NMR spectra of R-3 in chloroform (CDCl3). The red colours indicate the h...
Figure 2: a) R-3 gel in octane (5 mM); b) octane solution containing a mixture of R-3 (2.5 mM) and S-3 (2.5 m...
Figure 3: a) Concentration-dependent 1H NMR spectra of R-3 in cyclohexane-d12 and b) the shift of N–H signal ...
Figure 4: The evolution of ln(ee × 100) for the racemization of R-3 (1 mM) in the presence of 1 equivalent of...